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Peaks | tR (min) | Precursor Ion | Product Ion | Product Ion | |
---|---|---|---|---|---|
1. | Pregabalin | 1.24 | 160.2 | 142.1 | 55.0 |
2. | Gabapentin | 1.42 | 172.2 | 154.0 | 137.1 |
3. | Levetiracetam | 1.54 | 171.1 | 125.9 | 69.2 |
4. | Zonisamide | 1.98 | 212.9 | 132.1 | 77.1 |
5. | Felbamate | 2.03 | 239.1 | 117.1 | 177.8 |
6. | Lacosamide | 2.05 | 251.5 | 91.1 | 108.1 |
7. | Fosphenytoin | 2.29 | 363.1 | 265.9 | 207.8 |
Peaks | tR (min) | Precursor Ion | Product Ion | Product Ion | |
---|---|---|---|---|---|
8. | Topiramate | 2.30 | 340.2 | 264.2 | 223.9 |
9. | Ezogabine (Retigabine) | 2.30 | 304.0 | 230.1 | 109.1 |
10. | Phenytoin | 2.45 | 253.0 | 103.9 | 181.7 |
11. | Tiagabine | 2.49 | 376.2 | 246.8 | 111.1 |
12. | Eslicarbazepine | 2.62 | 297.2 | 237.1 | 194.0 |
13. | Clobazam | 2.90 | 301.0 | 259.1 | 224.0 |
14. | Perampanel | 3.31 | 350.2 | 219.1 | 247.1 |
Column | Raptor Biphenyl (cat.# 9309A12) | ||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||
Particle Size: | 2.7 µm | ||||||||||||||||||||||||
Guard Column: | Raptor Biphenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9309A0252) | ||||||||||||||||||||||||
Temp.: | 40 °C | ||||||||||||||||||||||||
Standard/Sample | |||||||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||||||
Conc.: | 25 ng/mL | ||||||||||||||||||||||||
Inj. Vol.: | 5 µL | ||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||
A: | Water + 0.1% formic acid | ||||||||||||||||||||||||
B: | Methanol + 0.1% formic acid | ||||||||||||||||||||||||
|
Detector | MS/MS |
---|---|
Ion Mode: | ESI+ |
Mode: | Scheduled MRM |
Instrument | UHPLC |
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