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Peaks | tR (min) | Conc. (ng/mL) | Precursor Ion | Product Ion | ESI Mode | |
---|---|---|---|---|---|---|
1. | Pitavastatin | 0.672 | 0.1 | 422.20 | 290.25 | + |
2. | Pravastatin | 0.805 | 5 | 423.25 | 321.20 | - |
3. | Rosuvastatin | 1.178 | 1 | 482.25 | 258.30 | + |
4. | Cerivastatin | 1.385 | 0.1 | 460.30 | 356.30 | + |
5. | Fluvastatin | 1.639 | 5 | 412.25 | 224.25 | + |
6. | Atorvastatin | 1.713 | 1 | 559.30 | 440.20 | + |
7. | Mevastatin | 1.964 | 1 | 413.15 | 311.35 | + |
8. | Lovastatin | 2.129 | 1 | 427.15 | 325.25 | + |
9. | Simvastatin | 2.316 | 1 | 441.25 | 325.40 | + |
Column | Raptor ARC-18 (cat.# 9314232) | ||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 30 mm x 2.1 mm ID | ||||||||||||||||||||||||
Particle Size: | 1.8 µm | ||||||||||||||||||||||||
Temp.: | 40 °C | ||||||||||||||||||||||||
Standard/Sample | |||||||||||||||||||||||||
Diluent: | 75:25 Water:acetonitrile | ||||||||||||||||||||||||
Conc.: | 0.1-5 ng/mL | ||||||||||||||||||||||||
Inj. Vol.: | 1 µL | ||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||
A: | 0.1% Formic acid in water | ||||||||||||||||||||||||
B: | 0.1% Formic acid in acetonitrile | ||||||||||||||||||||||||
|
Detector | MS/MS |
---|---|
Mode: | MRM |
Instrument | UHPLC |
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