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Drug and Drug Metabolites on Force Biphenyl by LC-MS/MS

LC_CF0778
PeakstR (min)Precursor IonProduct IonProduct Ion
1.Norcotinine1.35163.180.1118.0
2.Nicotine1.39163.2130.1117.1
3.BZP1.44177.291.165.1
4.Anabasine1.51163.292.1120.1
5.Normorphine1.56272.3165.1152.0
6.Noroxymorphone1.80288.2270.2213.2
7.Lisdexamfetamine1.82264.284.291.2
8.Cotinine2.02177.280.198.1
9.Psilocybin2.04285.3205.258.3
10.Dihydromorphine2.11288.3157.1185.0
11.Morphine2.16286.2152.1165.1
12.Morphine-6-β-D-glucuronide2.22462.3286.2201.1
13.Oxymorphone2.23302.2227.1198.1
14.Morphine-N-oxide2.31302.3285.2162.1
15.Hydromorphone2.41286.2185.1157.2
16.Psilocin2.42205.258.3160.1
17.Olanzapine2.66313.2256.1198.1
18.Methylephedrine2.68180.2162.2115.2
19.Norcodeine2.69286.1152.1115.0
20.Naloxone2.90328.3271.1310.1
21.Methamphetamine2.93150.391.1119.2
22.Noroxycodone2.98302.1284.2227.1
23.Dihydrocodeine2.98302.2199.2128.0
24.MDA2.98180.2163.1105.2
25.Codeine3.02300.2152.0165.0
26.O-Desmethyltramadol3.02250.144.0232.0
27.6-Acetylmorphine3.04328.2165.1211.2
28.Norhydrocodone3.05286.2199.1128.2
29.Phentermine3.07150.391.1133.2
30.Methylone3.07208.1160.2132.2
31.Desomorphine3.18272.1165.0152.2
32.Oxycodone3.19316.2298.2169.0
33.Naltrexone3.24342.2324.3267.2
34.Hydrocodone3.27300.2199.2128.2
35.Levamisole3.31205.1178.191.2
36.7-Aminonitrazepam3.34252.2121.194.2
37.O-Desmethylvenlafaxine3.38264.258.2107.0
38.MDEA3.54208.2163.2105.2
39.m-Hydroxybenzoylecgonine3.59306.2168.2121.1
40.Lamotrigine3.62256.1210.9145.0
41.N-Desmethyltapentadol3.63208.1107.2121.2
42.Tapentadol3.76222.2107.2121.2
43.Hydroxybupropion3.80256.0166.0130.2
44.Molindone3.81278.1100.170.1
45.Zolpidem Phenyl-4-carboxylic acid3.82338.2265.1219.0
46.Dextrorphan3.84258.2157.1201.2
47.Levorphanol3.84258.2157.2199.2
48.Tramadol3.86264.258.277.0
49.N-Desmethyltramadol3.98250.244.1232.1
50.Methylphenidate4.00234.484.256.1
51.Lacosamide4.03251.591.2108.2
52.Normeperidine4.06234.1160.291.0
53.Benzoylecgonine4.11290.2168.277.2
54.Remifentanil4.13377.4113.2317.2
55.Cocaine4.20304.2182.277.1
56.7-Aminoclonazepam4.24286.1121.2250.1
57.N-Desmethylclozapine4.25313.0192.1270.1
58.N-Desmethylmirtazapine4.27252.1195.2209.2
59.Norcocaine4.29290.1168.2136.2
60.MDPV4.29276.2126.3135.2
61.Pentazocine4.38286.2218.269.1
62.Mirtazapine4.40266.1195.2107.2
63.Butorphanol4.47328.3310.2131.0
64.Clozapine4.49328.2271.0193.0
PeakstR (min)Precursor IonProduct IonProduct Ion
65.Paliperidone4.51427.4207.2110.1
66.Iloperidone4.51427.1207.2110.2
67.9-Hydroxyrisperidone4.51427.0207.2110.2
68.Didemethylcitalopram4.73297.1109.2262.1
69.Citalopram4.75325.2109.2262.1
70.Escitalopram4.75325.3109.2262.1
71.Topiramate4.76340.0264.1224.0
72.Diphenhydramine4.76256.2167.2152.1
73.Haloperidol4.80377.2123.195.0
74.Desmethyldoxepin4.82266.1115.0107.2
75.Ezogabine4.84304.1109.2230.1
76.Fluoxetine4.91310.144.1148.0
77.Dextromethorphan5.01272.2215.2171.1
78.Chlordiazepoxide5.05300.1227.1282.0
79.Norpropoxyphene5.08326.4252.291.0
80.Propoxyphene5.09340.358.2266.3
81.Asenapine5.11286.2166.0229.0
82.Midazolam5.16326.1291.2223.0
83.Sufentanil5.16387.3238.2111.1
84.Protriptyline5.18264.1191.1165.0
85.Promazine5.19285.186.258.2
86.Amoxapine5.21314.2271.1193.1
87.Oxcarbazepine5.22253.1180.1208.1
88.Paroxetine5.23330.2192.270.2
89.Phenytoin5.24253.0182.2104.2
90.Loxapine5.25328.2271.1193.1
91.Maprotiline5.26278.1250.3191.1
92.Cyclobenzaprine5.26276.2215.1189.0
93.Amitriptyline5.27278.2202.191.2
94.EDDP5.27278.2234.1249.2
95.Venlafaxine5.27278.4260.2121.2
96.Nortriptyline5.29264.191.0115.0
97.Tenoxicam5.32338.1121.295.0
98.Trimipramine5.40295.2100.258.3
99.Pimozide5.43462.1109.2328.2
100.Mesoridazine5.44387.3126.198.2
101.α-Hydroxymidazolam5.48342.2324.1203.1
102.Clomipramine5.53315.386.258.2
103.Methadone5.55310.2265.2105.2
104.Sertraline5.56306.1158.9275.1
105.Metaxalone5.61222.1161.277.1
106.Eslicarbazepine5.65297.2194.2237.1
107.EMDP5.68264.2220.1235.2
108.N-Desmethylflunitrazepam5.82300.1254.1198.1
109.Ketorolac5.89256.1105.277.1
110.Etoricoxib5.95359.2280.1279.1
111.Clonazepam5.97316.1270.1214.1
112.Tolmetin6.03258.1119.291.1
113.Thioridazine6.03371.3126.398.2
114.α-Hydroxytriazolam6.04359.2331.1176.0
115.Methaqualone6.10251.1132.191.2
116.α-Hydroxyalprazolam6.17325.2297.1216.2
117.Clobazam6.28301.0259.1224.1
118.Parecoxib6.32371.2234.1165.0
119.Zaleplon6.32306.2236.1264.2
120.Flunitrazepam6.39314.2268.1239.1
121.Temazepam6.43301.1255.2283.1
122.Estazolam6.44295.1267.1205.1
123.Diazepam6.74285.1193.1154.2
124.XLR-117.02330.3125.1144.1
125.Prazepam7.04325.2271.2140.1
126.THC7.15315.2193.0123.1
127.JWH-0737.54328.2127.1155.1
128.JWH-0187.64342.3155.2127.1
ColumnForce Biphenyl (cat.# 962935E)
Dimensions:50 mm x 3.0 mm ID
Particle Size:3 µm
Pore Size:100 Å
Guard Column:Force Biphenyl EXP guard column cartridge 5 mm, 3 mm ID, 5 µm (cat.# 962950253)
Temp.:30 °C
Standard/Sample
Diluent:Water
Conc.:80 ng/mL
Inj. Vol.:1 µL
Mobile Phase
A:Water, 0.1% formic acid
B:Methanol, 0.1% formic acid
Time (min)Flow (mL/min)%A%B
0.000.8964
7.000.80100
8.000.80100
8.010.8964
10.000.8964
DetectorMS/MS
Ion Source:Electrospray
Ion Mode:ESI+
InstrumentUHPLC
Sample PreparationStandards were prepared in a 2 mL screw-thread vial (cat.# 21143) and capped with a short-cap, screw-vial closure (cat.#24498).
NotesThe analytical and guard columns were equipped with an UltraShield precolumn filter (cat. 25809).