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Peaks | tR (min) | Conc. (µg/mL) | |
---|---|---|---|
1. | Dalapon | 3.49 | 100 |
2. | Picloram | 5.98 | 100 |
3. | Dicamba | 8.68 | 100 |
4. | Chloramben | 9.04 | 100 |
5. | 4-Nitrophenol | 9.71 | 100 |
6. | 2,4-Dichlorophenylacetic acid | 12.53 | 40 |
7. | Bentazon | 12.70 | 100 |
8. | (4-Chloro-o-toloxy)acetic acid | 13.07 | 100 |
9. | 3,5-Dichlorobenzoic acid | 13.41 | 100 |
10. | 2,4-D | 13.49 | 100 |
11. | Mecoprop | 14.68 | 100 |
Peaks | tR (min) | Conc. (µg/mL) | |
---|---|---|---|
12. | Dichlorprop | 14.88 | 100 |
13. | 2,4,5-T | 15.66 | 100 |
14. | 2,4-DB | 15.83 | 100 |
15. | 2,4,5-TP | 16.73 | 100 |
16. | Phenol, pentachloro- | 19.42 | 100 |
17. | Acifluorfen | 19.47 | 100 |
18. | Dinoseb | 20.00 | 100 |
19. | 2,4-D Butoxyethyl ester | 20.78 | 200 |
20. | 2,4,5-T Butoxyethyl ester | 21.97 | 200 |
21. | 2,4,5-T Butyl ester | 22.29 | 200 |
22. | 2,4-D 2-Ethylhexyl ester | 24.12 | 200 |
Column | Ultra Cyano (cat.# 9106565) | ||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 150 mm x 4.6 mm ID | ||||||||||||
Particle Size: | 5 µm | ||||||||||||
Pore Size: | 100 Å | ||||||||||||
Temp.: | 30 °C | ||||||||||||
Standard/Sample | Chlorinated acids by HPLC, mix B (cat.# 32430) | ||||||||||||
Chlorinated acids by HPLC, mix A (cat.# 32431) | |||||||||||||
Dalapon (cat.# 32432) | |||||||||||||
2,4-Dichlorophenylacetic acid (cat.# 32439) | |||||||||||||
Diluent: | Water | ||||||||||||
Inj. Vol.: | 5 µL | ||||||||||||
Mobile Phase | |||||||||||||
A: | 0.05% H3PO4 in water | ||||||||||||
B: | Acetonitrile | ||||||||||||
|
Detector | UV/Vis @ 220, 0 nm |
---|---|
Instrument | Shimadzu UFLCXR |
Notes | Overlay of 5 injections 1. Black trace = cat.# 32430 2. Red trace = cat.# 32431 3. Purple trace = cat.# 32432 4. Green trace = cat.# 32439 5. Blue trace = metabolite mix |
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