Phenoxyacid Herbicides on Ultra Cyano (Overlay)

Column

Ultra Cyano (cat.# 9106565)

Dimensions:

150 mm x 4.6 mm ID

Particle Size:

5 µm

Pore Size:

100 Å

Temp.:

30 °C

Sample

Chlorinated acids by HPLC, mix B (cat.# 32430)

Chlorinated acids by HPLC, mix A (cat.# 32431)

Dalapon (cat.# 32432)

2,4-Dichlorophenylacetic acid (cat.# 32439)

Diluent:

Water

Inj. Vol.:

5 µL

Mobile Phase

0.05% H₃PO₄ in water

Acetonitrile

Time (min)	Flow (mL/min)	%A	%B
0.00	1	90	10
25	1	35	65

Detector	UV/Vis @ 220, 0 nm
Instrument	Shimadzu UFLCXR
Notes	Overlay of 5 injections 1. Black trace = cat.# 32430 2. Red trace = cat.# 32431 3. Purple trace = cat.# 32432 4. Green trace = cat.# 32439 5. Blue trace = metabolite mix

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