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Peaks | tR (min) | |
---|---|---|
1. | Formaldehyde | 1.516 |
2. | Acetaldehyde | 1.859 |
3. | Acetone | 2.283 |
4. | Acrolein | 2.461 |
5. | Propionaldehyde | 2.648 |
6. | Crotonaldehyde | 3.177 |
Peaks | tR (min) | |
---|---|---|
7. | Methyl ethyl ketone | 3.325 |
8. | Methacrolein | 3.474 |
9. | Butyraldehyde | 3.667 |
10. | Benzaldehyde | 4.069 |
11. | Valeraldehyde | 5.011 |
12. | m-Tolualdehyde | 5.239 |
13. | Hexaldehyde | 6.082 |
Column | Raptor ARC-18 (cat.# 9314A1E) | ||||||||||||||||||||||||
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Dimensions: | 100 mm x 3.0 mm ID | ||||||||||||||||||||||||
Particle Size: | 2.7 µm | ||||||||||||||||||||||||
Temp.: | 40 °C | ||||||||||||||||||||||||
Standard/Sample | CARB 1004 aldehyde/ketone-DNPH calibration standard (cat.# 33093) | ||||||||||||||||||||||||
Diluent: | Acetonitrile | ||||||||||||||||||||||||
Conc.: | 3 µg/mL | ||||||||||||||||||||||||
Inj. Vol.: | 3 µL | ||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||
A: | Water:tetrahydrofuran (5:2) | ||||||||||||||||||||||||
B: | Acetonitrile | ||||||||||||||||||||||||
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Max Pressure: | 240 bar |
Detector | UV/Vis @ 365, 4 nm |
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Notes | Using stainless steel tubing and fittings instead of PEEK material is recommended when the mobile phase contains high concentrations of tetrahydrofuran. |