Carbamate Pesticides on Ultra Carbamate by LC-MS/MS

	Peaks	t_R (min)	Precursor Ion	Product Ion	Product Ion
1.	Aldicarb sulfone	1.77	240.1	86.2	148.2
2.	Aldicarb sulfoxide	1.92	207.1	132.1	89.1
3.	Oxamyl	2.01	237.1	72.1	90.1
4.	Methomyl	2.22	163.1	106.0	88.1
5.	3-Hydroxycarbofuran	2.68	238.1	163.0	181.0
6.	Aldicarb	3.44	208.1	116.0	89.0
7.	Propoxur	3.71	210.1	111.0	168.1
8.	Carbofuran	3.80	222.1	165.1	123.0
9.	Carbaryl	4.07	202.1	145.0	127.0
10.	Methiocarb	4.78	226.1	169.1	121.1

Column

Ultra Carbamate (cat.# 9177312)

Dimensions:

100 mm x 2.1 mm ID

Particle Size:

3 µm

Pore Size:

100 Å

Temp.:

30 °C

Standard/Sample

531.1 Carbamate pesticide calibration mixture (cat.# 32273)

Diluent:

Water

Conc.:

10 ng/mL

Inj. Vol.:

5 µL

Mobile Phase

0.1% Formic acid + 5 mM ammonium formate in water

0.1% Formic acid + 5 mM ammonium formate in methanol

Time (min)	Flow (mL/min)	%A	%B
0.00	0.5	75	25
5.00	0.5	5	95
5.01	0.5	75	25
8.00	0.5	75	25

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