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Peaks | tR (min) | Precursor Ion | Product Ion | Product Ion | |
---|---|---|---|---|---|
1. | Aldicarb sulfone | 1.77 | 240.1 | 86.2 | 148.2 |
2. | Aldicarb sulfoxide | 1.92 | 207.1 | 132.1 | 89.1 |
3. | Oxamyl | 2.01 | 237.1 | 72.1 | 90.1 |
4. | Methomyl | 2.22 | 163.1 | 106.0 | 88.1 |
5. | 3-Hydroxycarbofuran | 2.68 | 238.1 | 163.0 | 181.0 |
6. | Aldicarb | 3.44 | 208.1 | 116.0 | 89.0 |
7. | Propoxur | 3.71 | 210.1 | 111.0 | 168.1 |
8. | Carbofuran | 3.80 | 222.1 | 165.1 | 123.0 |
9. | Carbaryl | 4.07 | 202.1 | 145.0 | 127.0 |
10. | Methiocarb | 4.78 | 226.1 | 169.1 | 121.1 |
Column | Ultra Carbamate (cat.# 9177312) | ||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||
Particle Size: | 3 µm | ||||||||||||||||||||
Pore Size: | 100 Å | ||||||||||||||||||||
Temp.: | 30 °C | ||||||||||||||||||||
Standard/Sample | 531.1 Carbamate pesticide calibration mixture (cat.# 32273) | ||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||
Conc.: | 10 ng/mL | ||||||||||||||||||||
Inj. Vol.: | 5 µL | ||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||
A: | 0.1% Formic acid + 5 mM ammonium formate in water | ||||||||||||||||||||
B: | 0.1% Formic acid + 5 mM ammonium formate in methanol | ||||||||||||||||||||
|
Detector | MS/MS |
---|---|
Ion Mode: | ESI+ |
Mode: | MRM |
Instrument | HPLC |
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