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Peaks | |
---|---|
1. | Aldicarb sulfone |
2. | Aldicarb sulfoxide |
3. | Oxamyl |
4. | Methomyl |
5. | 3-Hydroxycarbofuran |
Peaks | |
---|---|
6. | Aldicarb |
7. | Propoxur |
8. | Carbofuran |
9. | Carbaryl |
10. | Methiocarb |
11. | BDMC (IS) |
Column | Ultra Carbamate (cat.# 9177352) | ||||||||
---|---|---|---|---|---|---|---|---|---|
Dimensions: | 50 mm x 2.1 mm ID | ||||||||
Particle Size: | 3 µm | ||||||||
Pore Size: | 100 Å | ||||||||
Temp.: | ambient | ||||||||
Standard/Sample | 531.1 Carbamate Pesticide Calibration Mixture (cat.# 32273) | ||||||||
4-bromo-3,5-dimethylphenyl-N-methylcarbamate (BDMC) (cat.# 32274) | |||||||||
Diluent: | methanol | ||||||||
Conc.: | 10 ppm spiked into unprocessed orange oil | ||||||||
Inj. Vol.: | 3 µL | ||||||||
Mobile Phase | |||||||||
A: | 2 mM ammonium acetate:methanol, 90:10 | ||||||||
B: | 2 mM ammonium acetate:methanol, 10:90 | ||||||||
| |||||||||
Flow: | 0.2 mL/min |
Detector | LECO Unique® TOFMS |
---|---|
Ionization Source Type: | high flow ESI |
Ion Mode: | positive |
Nebulizing Pressure: | 100 kPa |
Desolvation Gas (N2): | 4 L/min |
Interface Temp.: | 120 °C |
Nozzle Voltage: | 62 V |
Capillary Voltage: | 2.75 kV |
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