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Peaks | |
---|---|
1. | Aldicarb sulfone |
2. | Aldicarb sulfoxide |
3. | Oxamyl |
4. | Methomyl |
5. | 3-Hydroxycarbofuran |
Peaks | |
---|---|
6. | Aldicarb |
7. | Propoxur |
8. | Carbofurane |
9. | Carbaryl |
10. | Methiocarb |
11. | BDMC (IS) |
Column | Ultra Carbamate (cat.# 9177352) | ||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 50 mm x 2.1 mm ID | ||||||||||||
Particle Size: | 3 µm | ||||||||||||
Pore Size: | 100 Å | ||||||||||||
Temp.: | ambient | ||||||||||||
Standard/Sample | 531.1 Carbamate Pesticide Calibration Mixture (cat.# 32273) | ||||||||||||
4-bromo-3,5-dimethylphenyl-N-methylcarbamate (BDMC) (cat.# 32274) | |||||||||||||
Diluent: | methanol | ||||||||||||
Conc.: | 50 µg/mL | ||||||||||||
Inj. Vol.: | 1 µL | ||||||||||||
Mobile Phase | |||||||||||||
A: | 2 mM ammonium acetate:methanol (v/v, 90/10) | ||||||||||||
B: | 2 mM ammonium acetate:methanol (v/v, 10/90) | ||||||||||||
| |||||||||||||
Flow: | 0.2 mL/min |
Detector | LECO Unique® TOFMS |
---|---|
Run Length: | 25 min |
Ionization Source Type: | high flow ESI |
Ion Mode: | positive |
Desolvation Temp.: | 130 °C |
Nebulizing Pressure: | 100 kPa |
Desolvation Gas (N2): | 4 L/min |
Interface Temp.: | 120 °C |
Nozzle Voltage: | 62 V |
Capillary Voltage: | 2.75 kV |
Instrument | Agilent 1100 |
Acknowledgement | LECO Corporation |
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