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Pesticides on Pinnacle DB Aqueous C18

LC_FF0479C
ColumnPinnacle DB Aqueous C18 (cat.# 9418252)
Dimensions:50 mm x 2.1 mm ID
Particle Size:1.9 µm
Pore Size:140 Å
Temp.:35 °C
Standard/Samplemulticomponent pesticide standard
Diluent:water
Conc.:33.3 ppb each pesticide
Inj. Vol.:5 µL
Mobile Phase
A:10mM NH4OAc in water
B:10mM NH4OAc in methanol
Time (min)%B
0.0010
110
890
1090
1110
Flow:0.60 mL/min
Max Pressure:~517 bar
DetectorApplied Biosystems/MDS Sciex LC/MS/MS
Model #:4000 QTRAP LC/MS/MS system
Ion Source:TurboIonSpray®
Ion Mode:ESI+
Ion Spray Voltage:5 kV
Gas 1:40 psi (275.8 kPa)
Gas 2:60 psi (413.7 kPa)
Source Temp.:500 °C
InstrumentShimadzu UFLCXR