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Peaks | tR (min) | Transition 1 | Transition 2 | |
---|---|---|---|---|
1. | Methamidophos | 1.06 | 142 -> 94 | 142 -> 125 |
2. | Acephate | 1.27 | 184.1 -> 143 | 184.1 -> 125 |
3. | Omethoate | 1.69 | 214 -> 124.9 | 214 -> 182.8 |
4. | Propamocarb | 6.61 | 189.2 -> 102.2 | 189.2 -> 73.9 |
Column | Ultra Aqueous C18 (cat.# 9178312) | ||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||
Particle Size: | 3 µm | ||||||||||||
Pore Size: | 100 Å | ||||||||||||
Temp.: | 35 °C | ||||||||||||
Standard/Sample | multicomponent pesticide standard | ||||||||||||
Diluent: | water | ||||||||||||
Conc.: | 1 ppb each pesticide | ||||||||||||
Inj. Vol.: | 10 µL | ||||||||||||
Mobile Phase | |||||||||||||
A: | 10 mM NH4OAc in water | ||||||||||||
B: | 10 mM NH4OAc in methanol | ||||||||||||
| |||||||||||||
Flow: | 0.5 mL/min |
Detector | Applied Biosystems/MDS Sciex LC/MS/MS |
---|---|
Model #: | 4000 QTRAP |
Ion Source: | TurboIonSpray® |
Ion Mode: | ESI+ |
Ion Spray Voltage: | 5 kV |
Gas 1: | 50 psi (344.7 kPa) |
Gas 2: | 60 psi (413.7 kPa) |
Source Temp.: | 600 °C |
Instrument | Shimadzu UFLCXR |
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