EU 15+1 PAHs on Pinnacle II PAH (FLD)

Column

Pinnacle II PAH, custom (cat.# 921946E)

Dimensions:

150 mm x 3.0 mm ID

Particle Size:

4 µm

Pore Size:

110 Å

Temp.:

30 °C

Standard/Sample

custom EU 15+1 PAH mix

Diluent:

acetonitrile

Conc.:

30 ng/mL (ppb)

Inj. Vol.:

5 µL

Mobile Phase

water

95:5 acetonitrile:tetrahydrofuran

Time (min)	Flow (mL/min)	%A	%B
0.00	1.5	30	70
3.00	1.5	25	75
10.00	1.5	0	100
14.50	1.5	0	100
14.51	1.5	30	70
16.50	1.5	30	70

Max Pressure:

275 bar

Detector

Shimadzu RF-10AXL

Time (min)	Wavelength Ex (nm)	Wavelength Em (nm)	Gain
0	270	390	1x
4.85	300	512	4x
5.80	290	430	1x
8.40	370	460	4x
8.90	290	430	1x
9.60	370	460	1x

Instrument

Shimadzu Prominence

Notes

RF-10AXL sensitivity: medium
Cyclopenta(c,d)pyrene was included in the EU 15+1 PAH mix but it does not fluoresce.

Download PDF