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Peaks | tR (min) | Precursor Ion (m/z) | Product Ion 1 (m/z) | Product Ion 2 (m/z) | |
---|---|---|---|---|---|
1. | Aldicarb sulfone | 3.5 | 240.1 | 86.2 | 148.2 |
2. | Butoxycarboxim | 3.5 | 223.1 | 106.0 | 166.0 |
3. | Aldicarb sulfoxide | 3.7 | 207.1 | 132.1 | 89.1 |
4. | Oxamyl | 3.8 | 237.1 | 72.1 | 90.1 |
5. | Methomyl | 3.9 | 163.1 | 106.0 | 88.1 |
6. | Aldicarb | 5.0 | 208.1 | 116.0 | 89.0 |
7. | Butocarboxim | 5.0 | 213.1 | 75.1 | 116.0 |
8. | Thidiazuron | 5.2 | 221.1 | 102.1 | 127.9 |
Peaks | tR (min) | Precursor Ion (m/z) | Product Ion 1 (m/z) | Product Ion 2 (m/z) | |
---|---|---|---|---|---|
9. | Thiophanate-methyl | 5.2 | 343.0 | 151.1 | 311.0 |
10. | Ethiofencarb | 5.6 | 226.1 | 107.2 | 164.0 |
11. | Tebuthiuron | 5.7 | 229.1 | 172.4 | 116.1 |
12. | Methabenzthiazuron | 6.5 | 222.1 | 165.2 | 150.3 |
13. | Methiocarb | 6.9 | 226.1 | 169.1 | 121.1 |
14. | Alanycarb | 9.2 | 400.1 | 238.1 | 90.9 |
15. | Benfuracarb | 10.2 | 411.2 | 190.0 | 252.1 |
16. | Furathiocarb | 10.3 | 383.1 | 195.1 | 252.1 |
Column | Ultra Aqueous C18 (cat.# 9178312) | ||||||||||||||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||||||||||||||
Particle Size: | 3 µm | ||||||||||||||||||||||||||||||||||||
Pore Size: | 100 Å | ||||||||||||||||||||||||||||||||||||
Temp.: | 50 °C | ||||||||||||||||||||||||||||||||||||
Standard/Sample | LC multiresidue pesticide standard #2 (cat.# 31973) | ||||||||||||||||||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||||||||||||||||||
Conc.: | 50 ng/mL | ||||||||||||||||||||||||||||||||||||
Inj. Vol.: | 20 µL | ||||||||||||||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||||||||||||||
A: | Water + 4 mM ammonium formate + 0.1% formic acid | ||||||||||||||||||||||||||||||||||||
B: | Methanol + 4 mM ammonium formate + 0.1% formic acid | ||||||||||||||||||||||||||||||||||||
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Max Pressure: | 255 bar |
Detector | AB SCIEX API 4000 LC-MS/MS |
---|---|
Ion Source: | TurboIonSpray® |
Ion Mode: | ESI+ |
Ion Spray Voltage: | 5.5 kV |
Curtain Gas: | 30 psi (206.8 kPa) |
Gas 1: | 40 psi (275.8 kPa) |
Gas 2: | 45 psi (310.3 kPa) |
CAD: | 10 psi (68.9 kPa) |
Source Temp.: | 350 °C |
Mode: | Scheduled MRM |
MRM Detection Window: | 60 sec |
Target Scan Time: | 0.33 sec |
Instrument | API LC-MS/MS |
Notes | Q1/Q3 Resolution: Unit Autosampler Temp.: 5 °C |
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