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LC Multiresidue Pesticide Standard #4 on Raptor ARC-18 by LC-MS/MS

LC_FF0546
PeakstR (min)Precursor IonProduct Ion 1Product Ion 2
1.Cyromazine1.07167.085.0108.1
2.Pymetrozine1.35218.0105.079.0
3.Dinotefuran1.63203.0129.0157.0
4.Nitenpyram1.68271.1125.9224.9
5.Flonicamid1.89230.0203.1174.1
6.Imidacloprid2.19256.1175.1209.1
7.Acetamiprid2.40223.0126.056.1
8.Cymoxanil2.47199.0128.0111.0
9.Oxadixyl2.77279.0219.0132.0
10.Carbetamide2.79237.0118.0192.0
11.Secbumeton2.93226.2100.2170.2
12.Prometon2.93226.086.3184.3
13.Terbumeton2.97226.1114.1170.1
14.Imazalil2.97297.0159.069.0
15.Pyracarbolid3.04218.1125.197.1
16.Ametryn3.22228.168.1186.1
17.Pyrimethanil3.51200.0107.082.0
18.Spiroxamine isomer 13.56298.0144.0100.0
19.Metalaxyl3.56280.1220.1192.1
20.Spiroxamine isomer 23.62298.0144.0100.0
21.Chlorantraniliprole3.66483.9286.0453.0
22.Azoxystrobin3.92404.1372.0329.0
23.Furalaxyl3.96302.1270.1242.2
24.Fludioxonil3.97249.1229.1158.1
25.Halofenozide3.98331.1104.9275.0
26.Boscalid4.06342.9307.0139.9
27.Mandipropamid4.08412.3328.2356.2
28.Flutolanil4.10324.1262.165.0
29.Mepronil4.20270.191.0119.0
30.Myclobutanil4.25289.1125.170.2
31.Methoxyfenozide4.29369.1149.1313.2
32.Triadimefon4.33294.1197.269.3
PeakstR (min)Precursor IonProduct Ion 1Product Ion 2
33.Cyprodinil4.34226.093.0108.0
34.Mepanipyrim4.40224.1106.077.0
35.Fenhexamid4.46302.197.255.3
36.Fluoxastrobin4.46459.0427.0188.0
37.Butafenacil4.48492.0180.0331.0
38.Picoxystrobin4.78368.0145.1205.1
39.Rotenone4.83395.0213.1192.1
40.Tebufenozide4.86353.1133.0297.1
41.Dimoxystrobin4.87327.1116.1205.2
42.Carfentrazone ethyl4.89412.0346.0266.0
43.Kresoxim-methyl4.90314.1206.0116.0
44.Zoxamide5.06336.0187.1159.0
45.Famoxadone5.09392.2331.1238.0
46.Prochloraz5.14376.0308.070.1
47.Benalaxyl5.15326.1148.091.0
48.Clofentezine5.21303.0138.0102.0
49.Benzoximate5.28364.0199.1105.0
50.Trifloxystrobin5.50409.0186.0145.0
51.Fluazinam5.77464.8373.0338.1
52.Metaflumizone5.79507.0287.2267.1
53.Tebufenpyrad5.85334.0117.0145.0
54.Pyriproxifen5.91322.196.0227.1
55.Piperonyl butoxide5.93356.3176.9119.0
56.Quinoxyfen6.03308.0197.0161.9
57.Amitraz6.14294.0163.0122.0
58.Fenpyroximate6.36422.2138.1366.1
59.Abamectin B1b6.47876.6553.4291.0
60.Eprinomectin6.53914.6186.0154.0
61.Abamectin B1a6.61890.5305.2567.3
62.Fenazaquin6.68307.2161.057.2
63.Doramectin6.81916.6331.2593.4
64.Moxidectin6.81640.5498.3528.4
65.Ivermectin7.00892.6569.4551.4
Isomers are numbered sequentially based on elution order.
ColumnRaptor ARC-18 (cat.# 9314A12)
Dimensions:100 mm x 2.1 mm ID
Particle Size:2.7 µm
Temp.:50 °C
Standard/SampleLC multiresidue pesticide standard #4 (cat.# 31975)
Diluent:Water
Conc.:20 ng/mL
Inj. Vol.:5 µL
Mobile Phase
A:Water + 2 mM ammonium formate + 0.2% formic acid
B:Methanol + 2 mM ammonium formate + 0.2% formic acid
Time (min)Flow (mL/min)%A%B
0.000.4955
2.000.44060
4.000.42575
6.000.40100
7.000.40100
7.010.4955
9.500.4955
DetectorWaters Xevo TQ-S
Ion Source:Waters Zspray™ ESI
Ion Mode:ESI+
Mode:MRM
InstrumentWaters
NotesAutosampler Temperature = 5 °C