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Peaks | tR (min) | Precursor Ion | Product Ion 1 | Product Ion 2 | |
---|---|---|---|---|---|
1. | Formetanate | 1.32 | 222.0 | 165.0 | 46.0 |
2. | Aminocarb | 1.34 | 209.0 | 137.0 | 152.0 |
3. | Propamocarb | 1.39 | 189.1 | 102.0 | 144.0 |
4. | Mexacarbate | 1.96 | 222.9 | 151.1 | 166.1 |
5. | Desmedipham | 3.54 | 318.0 | 182.0 | 154.0 |
6. | Phenmedipham | 3.62 | 301.0 | 168.0 | 136.0 |
7. | Pencycuron | 5.35 | 329.1 | 125.0 | 218.0 |
Column | Raptor ARC-18 (cat.# 9314A12) | ||||||||||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 100 mm x 2.1 mm ID | ||||||||||||||||||||||||||||||||
Particle Size: | 2.7 µm | ||||||||||||||||||||||||||||||||
Temp.: | 50 °C | ||||||||||||||||||||||||||||||||
Standard/Sample | LC multiresidue pesticide standard #9 (cat.# 31980) | ||||||||||||||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||||||||||||||
Conc.: | 20 ng/mL | ||||||||||||||||||||||||||||||||
Inj. Vol.: | 5 µL | ||||||||||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||||||||||
A: | Water + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
B: | Methanol + 2 mM ammonium formate + 0.2% formic acid | ||||||||||||||||||||||||||||||||
|
Detector | Waters Xevo TQ-S |
---|---|
Ion Source: | Waters Zspray™ ESI |
Ion Mode: | ESI+ |
Mode: | MRM |
Instrument | Waters |
Notes | Autosampler Temperature = 5 °C |
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