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|Column||Raptor Polar X (cat.# 9311A32)|
|Dimensions:||30 mm x 2.1 mm ID|
|Particle Size:||2.7 µm|
|Pore Size:||90 Å|
|Diluent:||15:85 Mobile phase A:mobile phase B|
|Inj. Vol.:||3 µL|
|A:||Water, 10 mM ammonium formate, 0.05% formic acid|
|B:||80:20 Acetonitrile:methanol, 0.05% formic acid|
|Detector||Shimadzu 8060 MS/MS|
|Instrument||Shimadzu Nexera X2|
|Sample Preparation||The sample was aliquoted into a 2.0 mL, 9 mm screw-thread polypropylene vial (cat.# 23242) and capped with a 9 mm solid-top polyethylene cap (cat.# 23244).|
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