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Analysis of Mycotoxins on Raptor FluoroPhenyl by LC-MS/MS

LC_FS0511
PeakstR (min)Conc.
(ng/mL)
Precursor IonProduct IonProduct Ion
1.Nivalenol1.04100313.22175.0991.08
2.Patulin1.4250155.0098.9480.98
3.Deoxynivalenol1.5350297.20249.04231.03
4.Fusarenon X2.13100355.20247.10175.08
5.15-Acetyldeoxynivalenol3.07100339.23321.15137.07
6.3-Acetyldeoxynivalenol3.22100339.16231.10213.08
7.Aflatoxin M14.1125329.22273.09229.12
8.Diacetoxyscirpenol4.41100367.24307.14105.07
9.Aflatoxin G24.6725331.16313.00189.01
10.Aflatoxin G14.8725329.13243.00199.74
11.HT-24.9250447.20345.08285.11
12.Aflatoxin B25.2025315.13287.02258.98
13.Aflatoxin B15.3225313.16284.85241.06
14.Citrinin5.3810251.15233.09205.05
15.Fumonisin B15.5625722.46352.25334.23
16.T-25.6350489.24245.07387.12
17.Fumonisin B36.0325706.43336.23318.29
18.Ochratoxin A6.1725404.07238.96357.98
19.Fumonisin B26.3125706.43336.23318.29
20.Zearalenone6.4450319.23283.06187.04
ColumnRaptor FluoroPhenyl (cat.# 9319A12)
Dimensions:100 mm x 2.1 mm ID
Particle Size:2.7 µm
Pore Size:90 Å
Guard Column:Raptor FluoroPhenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9319A0252)
Temp.:30 °C
Sample
Diluent:Water:methanol (80:20)
Conc.:10-100 ng/mL
Inj. Vol.:5 µL
Mobile Phase
A:0.3% Formic acid in water
B:Methanol
Time (min)Flow (mL/min)%A%B
0.000.48020
7.000.41090
7.010.48020
9.000.48020
Max Pressure:525 bar
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentUHPLC