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Mycotoxins in Solvent on Raptor Biphenyl by LC-MS/MS

LC_FS0523
PeakstR (min)Conc.
(ng/g)
Precursor IonProduct Ion 1Product Ion 2
1.Deoxynivalenol0.64150297.3249.3231.2
2.Deoxynivalenol-13C150.64125312.3263.3245.2
3.Fumonisin B12.45150722.5352.4334.5
4.HT-22.59150447.3285.3345.3
5.Fumonisin B32.85150706.5336.4318.4
6.Fumonisin B23.23150706.5336.3141.2
7.T-23.31150489.3245.2387.4
8.Aflatoxin G23.7415331.2313.3189.3
9.Aflatoxin G2-13C173.7425348.3330.3200.4
PeakstR (min)Conc.
(ng/g)
Precursor IonProduct Ion 1Product Ion 2
10.Zearalenone3.96150319.3283.3187.2
11.Aflatoxin G14.2215329.2243.2200.2
12.Aflatoxin G1-13C174.2225346.3257.3212.3
13.Aflatoxin B24.4315315.3287.3259.2
14.Aflatoxin B2-13C174.4325332.3303.3273.3
15.Aflatoxin B14.9915313.3285.2241.2
16.Aflatoxin B1-13C174.9925330.3301.4255.3
17.Ochratoxin A5.1915404.2239.3358.3
18.Ochratoxin A-13C205.1920424.3250.2377.2
ColumnRaptor Biphenyl (cat.# 9309A52)
Dimensions:50 mm x 2.1 mm ID
Particle Size:2.7 µm
Pore Size:90 Å
Guard Column:Raptor Biphenyl EXP guard column cartridge 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9309A0252)
Temp.:40 °C
Sample
Diluent:65:35 Water:methanol
Inj. Vol.:5 µL
Mobile Phase
A:Water, 2 mM ammonium formate, 0.1% formic acid
B:Methanol, 2 mM ammonium formate, 0.1% formic acid
Time (min)Flow (mL/min)%A%B
0.000.57030
0.60.57030
0.70.55050
3.00.53070
4.50.52575
5.00.51090
5.20.51090
5.210.52575
6.000.52575
6.010.57030
7.000.57030
DetectorMS/MS
Ion Mode:ESI+
Mode:MRM
InstrumentUHPLC