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Peaks | tR (min) | Conc. (ng/mL) | Precursor Ion | Product Ion 1 | Product Ion 2 | Product Ion 3 | Precursor 2 | Product Ion 2 | |
---|---|---|---|---|---|---|---|---|---|
1. | Aminomethylphosphonic acid (AMPA) | 0.805 | 200 | 110.1 | 79.1 | 63.1 | 81.1 | - | - |
2. | Bialophos | 0.847 | 100 | 322.2 | 88.2 | 216.1 | 134.2 | - | - |
3. | Perchlorate | 2.593 | 5 | 101.0 | 84.95 | - | - | 98.9 | 83 |
4. | Glufosinate | 3.376 | 200 | 180.2 | 85.2 | 95.1 | - | - | - |
5. | 3-(Methylphophinico) propionic acid (MPPA) | 4.076 | 100 | 151.0 | 63.0 | 107.1 | 133.2 | - | - |
6. | Trifluoracetic acid (TFA) | 4.423 | 20 | 113.0 | 69.1 | 19.1 | - | - | - |
7. | 2-Hydroxyethane phosphonic acid (HEPA) | 4.969 | 100 | 125.1 | 79.0 | 95.0 | 63 | - | - |
8. | Difluoroacetic acid (DFA) | 5.018 | 200 | 95.0 | 51.1 | - | - | - | - |
9. | Chlorate | 5.542 | 100 | 85.0 | 69.0 | - | - | 83.0 | 67.1 |
10. | Ethephon | 5.564 | 200 | 143.1 | 107.2 | - | - | - | |
11. | Glyphosate | 6.113 | 200 | 168.1 | 63.1 | 79.1 | - | - | - |
12. | Bromide | 6.423 | 2000 | 80.9 | 80.9 | - | - | 79.0 | 79.0 |
13. | Bromate | 6.771 | 600 | 129.0 | 113 | - | - | 127 | 111.1 |
14. | N-acetyl AMPA | 6.932 | 200 | 152.1 | 110.1 | 62.9 | - | - | - |
15. | Fosetyl aluminum | 7.775 | 80 | 109.1 | 81.0 | 63.0 | 78.9 | - | - |
16. | Phosphonic acid | 8.275 | 500 | 81.1 | 62.9 | - | - | - | - |
17. | N-acetyl glufosinate | 9.980 | 200 | 222.2 | 136.1 | 134.1 | 59.0 | - | - |
Column | Raptor Polar X (cat.# 9311A32) | ||||||||||||||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 30 mm x 2.1 mm ID | ||||||||||||||||||||||||
Particle Size: | 2.7 µm | ||||||||||||||||||||||||
Pore Size: | 90 Å | ||||||||||||||||||||||||
Temp.: | 35 °C | ||||||||||||||||||||||||
Standard/Sample | |||||||||||||||||||||||||
Diluent: | Water | ||||||||||||||||||||||||
Inj. Vol.: | 1 µL | ||||||||||||||||||||||||
Mobile Phase | |||||||||||||||||||||||||
A: | Water, 0.5% formic acid | ||||||||||||||||||||||||
B: | Acetonitrile, 0.5% formic acid | ||||||||||||||||||||||||
|
Detector | MS/MS |
---|---|
Ion Mode: | ESI- |
Mode: | MRM |
Instrument | UHPLC |
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