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Peaks | tR (min) | Conc. (µg/mL) | |
---|---|---|---|
1. | Cannabidivarinic acid (CBDVA) | 1.500 | 50 |
2. | Cannabidivarin (CBDV) | 1.650 | 50 |
3. | Cannabidiolic acid (CBDA) | 2.060 | 50 |
4. | Cannabigerolic acid (CBGA) | 2.195 | 50 |
5. | Cannabigerol (CBG) | 2.305 | 50 |
6. | Cannabidiol (CBD) | 2.420 | 50 |
7. | Tetrahydrocannabivarin (THCV) | 2.635 | 50 |
8. | Tetrahydrocannabivarinic acid (THCVA) | 3.330 | 50 |
Peaks | tR (min) | Conc. (µg/mL) | |
---|---|---|---|
9. | Cannabinol (CBN) | 3.570 | 50 |
10. | Cannabinolic acid (CBNA) | 4.270 | 50 |
11. | Delta-9-Tetrahydrocannabinol (Δ9-THC) | 4.480 | 50 |
12. | Delta-8-Tetrahydrocannabinol (Δ8-THC) | 4.630 | 50 |
13. | Cannabicyclol (CBL) | 5.320 | 50 |
14. | Cannabichromene (CBC) | 5.605 | 50 |
15. | Tetrahydrocannabinolic acid A (THCA-A) | 5.890 | 50 |
16. | Cannabichromenic acid (CBCA) | 6.650 | 50 |
Column | Raptor ARC-18 (cat.# 9314A62) | ||||||||||||
---|---|---|---|---|---|---|---|---|---|---|---|---|---|
Dimensions: | 150 mm x 2.1 mm ID | ||||||||||||
Particle Size: | 2.7 µm | ||||||||||||
Pore Size: | 90 Å | ||||||||||||
Guard Column: | Raptor ARC-18 5 mm, 2.1 mm ID, 2.7 µm (cat.# 9314A0252) | ||||||||||||
Temp.: | 30 °C | ||||||||||||
Standard/Sample | Cannabinoids acids 7 standard (cat.# 34144) | ||||||||||||
Cannabinoids neutrals 9 standard (cat.# 34132) | |||||||||||||
Diluent: | Acetonitrile | ||||||||||||
Conc.: | 50 ppm | ||||||||||||
Inj. Vol.: | 2 µL | ||||||||||||
Mobile Phase | |||||||||||||
A: | Water, 5 mM ammonium formate, 0.1% formic acid | ||||||||||||
B: | Acetonitrile, 0.1% formic acid | ||||||||||||
|
Detector | UV/Vis @ 228 nm |
---|---|
Instrument | UHPLC |
Sample Preparation | Standards were aliquoted into 2 mL, screw-thread vials (cat.# 21143) and capped with short-cap, screw-vial closures (cat.# 24498). |
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